1ULU
Crystal structure of tt0143 from Thermus thermophilus HB8
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL26B1 |
Synchrotron site | SPring-8 |
Beamline | BL26B1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2002-07-09 |
Detector | RIGAKU JUPITER |
Wavelength(s) | 0.965, 0.9795, 0.9791 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 97.033, 96.706, 107.639 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.200 - 2.000 |
R-factor | 0.218 |
Rwork | 0.218 |
R-free | 0.24900 |
Structure solution method | MAD |
RMSD bond length | 0.005 |
RMSD bond angle | 1.200 |
Data reduction software | MOSFLM |
Data scaling software | CCP4 ((SCALA)) |
Phasing software | SOLVE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.200 | 2.110 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.087 | 0.385 |
Number of reflections | 68642 | |
<I/σ(I)> | 5.8 | 1.7 |
Completeness [%] | 99.4 | 96.4 |
Redundancy | 6.1 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | VAPOR DIFFUSION, HANGING DROP, temperature 293.0K |