1UDB
STRUCTURE OF UDP-GALACTOSE-4-EPIMERASE COMPLEXED WITH UDP-4-DEOXY-4-FLUORO-ALPHA-D-GLUCOSE
Experimental procedure
Spacegroup name | P 32 2 1 |
Unit cell lengths | 83.500, 83.500, 108.900 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 30.000 - 1.650 |
R-factor | 0.179 * |
Rwork | 0.179 |
RMSD bond length | 0.010 |
RMSD bond angle | 2.150 |
Refinement software | TNT |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 1.730 | |
High resolution limit [Å] | 1.650 * | 1.650 |
Rmerge | 0.051 | 0.230 |
Total number of observations | 124280 * | |
Number of reflections | 49619 | 5317 * |
Completeness [%] | 93.0 | 81 |
Redundancy | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 9 * | 4 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | PEG8000 | 20-25 (%) | |
2 | 1 | reservoir | 250-500 (mM) | ||
3 | 1 | reservoir | CHES | 50 (mM) |