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1U7R

Crystal structure of Native Sperm Whale myoglobin from low ionic strength enviroment (Form2 )

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 14-BM-D
Synchrotron siteAPS
Beamline14-BM-D
Temperature [K]100
Detector technologyCCD
Collection date2000-01-01
DetectorADSC QUANTUM 4
Wavelength(s)1
Spacegroup nameP 21 21 21
Unit cell lengths39.950, 47.974, 78.332
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution40.000 - 1.150
R-factor0.1376
Rwork0.138
R-free0.16470
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.019
RMSD bond angle0.035
Data reduction softwareHKL-2000
Data scaling softwareSCALEPACK
Phasing softwareSHELX
Refinement softwareSHELXL-97
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]40.0001.190
High resolution limit [Å]1.1501.150
Rmerge0.0390.235
Number of reflections53703
<I/σ(I)>2.8
Completeness [%]100.092.8
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP727750mM imidazole, pH 7 with 16% PEG3550, VAPOR DIFFUSION, HANGING DROP, temperature 277K

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