1U76
Crystal structure of hPCNA bound to residues 452-466 of the DNA polymerase-delta-p66 subunit
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CHESS BEAMLINE A1 |
Synchrotron site | CHESS |
Beamline | A1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-02-29 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.9764 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 82.480, 82.480, 203.800 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 10.000 - 2.600 |
R-factor | 0.24 |
Rwork | 0.240 |
R-free | 0.27800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB 1AXC.pdb without chains B D F |
RMSD bond length | 0.007 |
RMSD bond angle | 1.300 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.690 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.082 | 0.336 |
Number of reflections | 24477 | |
<I/σ(I)> | 7.4 | 3.8 |
Completeness [%] | 96.0 | 100 |
Redundancy | 4.36 | 5.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 298 | ammonium sulfate, sodium acetate, pH 4.6, VAPOR DIFFUSION, HANGING DROP, temperature 298K |