1U65
Ache W. CPT-11
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RUH3R |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2004-02-25 |
| Detector | RIGAKU RAXIS4++ |
| Spacegroup name | P 32 2 1 |
| Unit cell lengths | 137.870, 137.870, 70.890 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 27.880 - 2.610 |
| R-factor | 0.187 |
| Rwork | 0.187 |
| R-free | 0.23700 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.300 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | CNS |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 28.000 | 2.700 |
| High resolution limit [Å] | 2.600 | 2.600 |
| Rmerge | 0.094 | 0.211 |
| Number of reflections | 23820 | |
| <I/σ(I)> | 10.3 | 4.7 |
| Completeness [%] | 98.5 | 90.9 |
| Redundancy | 3.17 | 2.98 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7.5 | pH 7.5 |
