1U0R
Crystal structure of Mycobacterium tuberculosis NAD kinase
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-04-20 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.9793,0.9795,0.9392 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 118.510, 118.510, 222.300 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.800 |
R-factor | 0.224 |
Rwork | 0.223 |
R-free | 0.28600 |
Structure solution method | MAD |
RMSD bond length | 0.018 |
RMSD bond angle | 1.889 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SHELXS |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.800 |
Number of reflections | 38743 |
Completeness [%] | 99.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.6 | 298 | lithium sulfate, ammonium sulfate, sodium citrate, pH 5.6, VAPOR DIFFUSION, HANGING DROP, temperature 298K, pH 5.60 |