1U0L
Crystal structure of YjeQ from Thermotoga maritima
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Temperature [K] | 90 |
Detector technology | CCD |
Collection date | 2004-04-25 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.9793 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 142.819, 114.798, 77.088 |
Unit cell angles | 90.00, 105.72, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.800 |
R-factor | 0.218 |
Rwork | 0.218 |
R-free | 0.28400 |
Structure solution method | SAD |
RMSD bond length | 0.007 |
RMSD bond angle | 1.500 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 |
High resolution limit [Å] | 2.800 | 2.800 |
Number of reflections | 29551 | |
Completeness [%] | 100.0 | 100 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 295 | 15% PEG3350, 0.2M KCL, 10mM Guanidine HCl, 0.1M Tris, pH 8, VAPOR DIFFUSION, HANGING DROP, temperature 295K |