1U0K
The structure of a Predicted Epimerase PA4716 from Pseudomonas aeruginosa
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 150 |
Detector technology | CCD |
Collection date | 2004-04-19 |
Detector | CUSTOM-MADE |
Wavelength(s) | 0.97959 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 39.778, 69.477, 94.950 |
Unit cell angles | 90.00, 101.10, 90.00 |
Refinement procedure
Resolution | 91.290 - 1.500 |
R-factor | 0.16827 |
Rwork | 0.167 |
R-free | 0.18867 |
Structure solution method | SAD |
RMSD bond length | 0.009 |
RMSD bond angle | 1.193 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SOLVE |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.570 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.371 | |
Number of reflections | 75759 | |
<I/σ(I)> | 5.74 | |
Completeness [%] | 98.2 | 97.3 |
Redundancy | 7.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5 | 298 | di-Ammonium Citrate, PEG 3350, sucrose, VAPOR DIFFUSION, HANGING DROP, temperature 298K |