1TZU
T. maritima NusB, P212121
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MPG/DESY, HAMBURG BEAMLINE BW6 |
Synchrotron site | MPG/DESY, HAMBURG |
Beamline | BW6 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2002-04-01 |
Detector | MARRESEARCH |
Wavelength(s) | 1.05 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 33.766, 59.600, 64.322 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.850 |
R-factor | 0.22575 |
Rwork | 0.224 |
R-free | 0.25253 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB ID 1EYV |
RMSD bond length | 0.010 |
RMSD bond angle | 1.015 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC (5.1.19) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.950 |
High resolution limit [Å] | 1.850 | 1.850 |
Number of reflections | 11016 | |
<I/σ(I)> | 20.6 | 3.1 |
Completeness [%] | 94.6 | 94.8 |
Redundancy | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.4 | 293 | 2-propanol, PEG 4000, pH 7.4, VAPOR DIFFUSION, SITTING DROP, temperature 293K |