1TZA
X-ray structure of Northeast Structural Genomics Consortium target SoR45
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X4A |
Synchrotron site | NSLS |
Beamline | X4A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-06-24 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.97868 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 51.947, 72.287, 75.574 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.670 - 2.400 |
R-factor | 0.221 |
Rwork | 0.217 |
R-free | 0.26800 |
Structure solution method | SAD |
RMSD bond length | 0.006 |
RMSD bond angle | 1.400 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.490 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.050 | 0.073 |
Number of reflections | 10666 | |
<I/σ(I)> | 52.23 | 37.83 |
Completeness [%] | 92.3 | 99.1 |
Redundancy | 8.93 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5 | 8% PEG4000, 0.05mM Cacodylic Acid, pH 5.0, VAPOR DIFFUSION, HANGING DROP |