1TYR

TRANSTHYRETIN COMPLEX WITH RETINOIC ACID

Experimental procedure

Detector technology	AREA DETECTOR
Collection date	1994-11
Detector	SIEMENS-NICOLET X100
Spacegroup name	P 21 21 2
Unit cell lengths	43.800, 86.220, 65.780
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	9.000 - 1.800
R-factor	0.196
RMSD bond length	0.010 *
RMSD bond angle	3.500 *
Data reduction software	SAINT
Refinement software	TNT

Data quality characteristics

	Overall
Rmerge	0.070
Redundancy	3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, sitting drop *	7 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	ammonium sulfate	2 (M)
2	1	reservoir	sodium citrate	0.2 (M)