1TYM

THE STRUCTURE OF A COMPLEX OF HEXAMERIC INSULIN AND 4'-HYDROXYACETANILIDE

Experimental procedure

Spacegroup name	H 3
Unit cell lengths	80.880, 80.880, 37.600
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	8.000 * - 1.900
R-factor	0.173
RMSD bond length	0.019
RMSD bond angle	0.046 *
Refinement software	PROFFT

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	9999.000 *
High resolution limit [Å]	1.800 *	1.800 *
Rmerge	0.061 *
Total number of observations	44075 *
Number of reflections	7866 *
Completeness [%]		37 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	Tylenol	0.07 (M)
2	1	1		1.0 (M)
3	1	1	sodium citrate	0.05 (M)
4	1	1	zinc acetate	0.007 (M)
5	1	1	4'-hydroxyacetanilide	0.07 (M)
6	1	1	sodium chloride	0.75 (M)