1TXY
E. coli PriB
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.3.1 |
Synchrotron site | ALS |
Beamline | 8.3.1 |
Temperature [K] | 110 |
Detector technology | CCD |
Collection date | 2004-06-10 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 1.0200, 0.9798, 0.9797 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 49.902, 60.294, 66.304 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.000 |
R-factor | 0.26009 |
Rwork | 0.259 |
R-free | 0.28485 |
Structure solution method | MAD |
RMSD bond length | 0.012 |
RMSD bond angle | 1.147 |
Data reduction software | MOSFLM |
Data scaling software | CCP4 ((SCALA)) |
Phasing software | SOLVE |
Refinement software | REFMAC (5.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 34.000 | 2.100 |
High resolution limit [Å] | 2.000 | 2.000 |
Number of reflections | 16070 | |
Completeness [%] | 99.9 | 99.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 298 | PEG 8000, Tris-HCl, pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |