1TWE
INTERLEUKIN 1 BETA MUTANT F101Y
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Collection date | 1999-10-25 |
Detector | RIGAKU |
Wavelength(s) | 1.5418 |
Spacegroup name | P 43 |
Unit cell lengths | 55.000, 55.000, 77.000 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 77.000 - 2.100 |
Rwork | 0.184 |
R-free | 0.20060 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 77.000 | 2.150 |
High resolution limit [Å] | 2.100 | 2.100 |
Number of reflections | 13397 | |
Completeness [%] | 99.8 | 99.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.4 | 298 | 100 mM TRIS, 29% W/V AMMONIUM SULFATE, pH 7.4, VAPOR DIFFUSION, HANGING DROP, temperature 298K |