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1TW9

Glutathione Transferase-2, apo form, from the nematode Heligmosomoides polygyrus

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsCHESS BEAMLINE A1
Synchrotron siteCHESS
BeamlineA1
Temperature [K]100
Detector technologyCCD
Collection date2002-10-07
DetectorADSC QUANTUM 210
Wavelength(s)0.947
Spacegroup nameP 1
Unit cell lengths72.678, 74.034, 88.573
Unit cell angles79.09, 80.08, 81.55
Refinement procedure
Resolution25.000 - 1.710
R-factor0.18132
Rwork0.180
R-free0.23198
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1PD2 (Prostaglandin D synthase)
RMSD bond length0.019
RMSD bond angle1.798
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareBEAST
Refinement softwareREFMAC (5.1.9999)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]25.0001.760
High resolution limit [Å]1.7001.700
Rmerge0.0670.394
Number of reflections184048
<I/σ(I)>12.62
Completeness [%]95.981.4
Redundancy6.22.8
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP8.5292PEG 20K, calcium chloride, Tris-HCL, pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 292K

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