1TUL

STRUCTURE OF TLP20

Experimental procedure

Collection date	1992-09
Detector	SIEMENS
Spacegroup name	P 21 3
Unit cell lengths	76.300, 76.300, 76.300
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	30.000 - 2.200
R-factor	0.181 *
Rwork	0.181
RMSD bond length	0.014
RMSD bond angle	18.700 *
Data reduction software	XDS
Refinement software	TNT

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000 *
High resolution limit [Å]	2.200 *	2.200 *
Rmerge	0.048	0.242 *
Total number of observations	36733 *
Number of reflections	7732 *	927 *
Completeness [%]	99.8
Redundancy	4.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	6 *		macroseeding *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	ammonium sulfate	0.8-0.9 (M)
2	1	drop		0.25 (mM)
3	1	drop	Na+/K+ succinate
4	1	reservoir	ammonium sulfate	1.8 (M)