1TUH
Structure of Bal32a from a Soil-Derived Mobile Gene Cassette
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | ENRAF-NONIUS |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2003-07-25 |
Detector | MARRESEARCH |
Wavelength(s) | 1.5418 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 60.728, 60.728, 89.910 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 22.470 - 1.850 |
R-factor | 0.18689 |
Rwork | 0.185 |
R-free | 0.21213 |
Structure solution method | MIR |
RMSD bond length | 0.020 |
RMSD bond angle | 1.752 |
Data reduction software | MOSFLM |
Data scaling software | CCP4 ((SCALA)) |
Phasing software | MLPHARE |
Refinement software | REFMAC (5.2.0003) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 22.500 | 1.898 |
High resolution limit [Å] | 1.850 | 1.850 |
Number of reflections | 14962 | |
Completeness [%] | 100.0 | 100 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.6 | 291 | ammonium sulfate, sodium acetate, pH 4.6, VAPOR DIFFUSION, SITTING DROP, temperature 291K |