1TU4
Crystal Structure of Rab5-GDP Complex
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | CAMD BEAMLINE GCPCC |
Synchrotron site | CAMD |
Beamline | GCPCC |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-01-12 |
Detector | MARRESEARCH |
Wavelength(s) | 0.9798,0.9794,0.9253 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 84.900, 84.900, 199.900 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.610 - 2.200 |
R-factor | 0.217 |
Rwork | 0.217 |
R-free | 0.27400 |
Structure solution method | MAD |
RMSD bond length | 0.007 |
RMSD bond angle | 1.000 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS (1.1) |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.280 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.058 | 0.378 |
Number of reflections | 42778 | |
<I/σ(I)> | 32.6 | 3.4 |
Completeness [%] | 98.8 | 89.6 |
Redundancy | 8.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | ammonium sulfate, cobalt chloride, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |