1TTI
THREE NEW CRYSTAL STRUCTURES OF POINT MUTATION VARIANTS OF MONOTIM: CONFORMATIONAL FLEXIBILITY OF LOOP-1,LOOP-4 AND LOOP-8
Experimental procedure
Spacegroup name | C 1 2 1 |
Unit cell lengths | 78.780, 46.760, 70.390 |
Unit cell angles | 90.00, 113.99, 90.00 |
Refinement procedure
Resolution | 32.000 - 2.400 |
R-factor | 0.178 * |
Rwork | 0.178 |
RMSD bond length | 0.020 |
RMSD bond angle | 2.300 * |
Phasing software | X-PLOR |
Refinement software | TNT |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 32.000 | |
High resolution limit [Å] | 2.400 | 2.400 * |
Rmerge | 0.065 * | |
Total number of observations | 11293 * | |
Number of reflections | 7034 | |
Completeness [%] | 75.0 * | 25 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | MES | 100 (mM) | |
2 | 1 | drop | DTT | 1 (mM) | |
3 | 1 | drop | EDTA | 1 (mM) | |
4 | 1 | drop | 1 (mM) | ||
5 | 1 | drop | 2PG | 3 (mM) | |
6 | 1 | reservoir | PEG6000 | 22 (%) |