1TS6
Structure of the pB2 intermediate from time-resolved Laue crystallography
Experimental procedure
| Experimental method | LAUE |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 14-ID-B |
| Synchrotron site | APS |
| Beamline | 14-ID-B |
| Temperature [K] | 288 |
| Spacegroup name | P 63 |
| Unit cell lengths | 66.833, 66.833, 40.947 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 30.000 - 1.600 |
| R-factor | 0.1813 |
| Rwork | 0.175 |
| R-free | 0.18620 |
| Structure solution method | Difference Fourier |
| Data reduction software | LaueView |
| Data scaling software | LaueView |
| Refinement software | SHELXL-97 |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 30.000 |
| High resolution limit [Å] | 1.600 |
| Number of reflections | 13891 |
| Completeness [%] | 100.0 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | 2.6 M ammonium sulfate, 50 mM sodium phosphate, pH 7, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
