1TRD
THE INFLUENCE OF CRYSTAL PACKING ON CRYSTALLOGRAPHIC BINDING STUDIES: A NEW CRYSTAL FORM OF TRYPANOSOMAL TIM
Experimental procedure
Spacegroup name | C 1 2 1 |
Unit cell lengths | 94.620, 48.000, 131.310 |
Unit cell angles | 90.00, 100.33, 90.00 |
Refinement procedure
Resolution | ? - 2.500 |
R-factor | 0.147 |
Rwork | 0.147 |
RMSD bond length | 0.014 |
RMSD bond angle | 2.500 * |
Phasing software | X-PLOR |
Refinement software | TNT |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.500 * |
Rmerge | 0.057 * |
Total number of observations | 26995 * |
Number of reflections | 18801 * |
Completeness [%] | 69.7 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 7.6 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | TIM | 5 (mg/ml) | |
10 | 1 | reservoir | dithiothreitol | 1 (mM) | |
11 | 1 | reservoir | EDTA | 1 (mM) | |
12 | 1 | reservoir | 1 (mM) | ||
2 | 1 | drop | Tris/Hcl | 25 (mM) | |
3 | 1 | drop | 20 (mM) | ||
4 | 1 | drop | ammonium | 50 (mM) | |
5 | 1 | drop | EDTA | 1 (mM) | |
6 | 1 | drop | dithiothreitol | 1 (mM) | |
7 | 1 | drop | 1 (mM) | ||
8 | 1 | reservoir | PEG6000 | 18 (%) | |
9 | 1 | reservoir | Tris/HCl | 200 (mM) |