1TQ5
Crystal Structure of YhhW from Escherichia coli
Experimental procedure
| Experimental method | SAD |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-BM |
| Synchrotron site | APS |
| Beamline | 19-BM |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2003-11-12 |
| Detector | SBC-3 |
| Wavelength(s) | 0.98027 |
| Spacegroup name | P 32 2 1 |
| Unit cell lengths | 62.769, 62.769, 98.053 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 54.230 - 1.760 |
| R-factor | 0.20449 |
| Rwork | 0.197 |
| R-free | 0.25030 |
| Structure solution method | SAD |
| RMSD bond length | 0.038 |
| RMSD bond angle | 2.724 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | SOLVE |
| Refinement software | REFMAC (5.0) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 54.230 | 1.809 |
| High resolution limit [Å] | 1.760 | 1.763 |
| Number of reflections | 19955 | |
| Completeness [%] | 54.25 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 295 | PEG 400, sodium acetate, cadmium chloride, pH 4.6, VAPOR DIFFUSION, HANGING DROP, temperature 295K |
