1TPW

TRIOSEPHOSPHATE ISOMERASE DRINKS WATER TO KEEP HEALTHY

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	136.200, 74.300, 53.500
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	6.000 * - 1.940 *
R-factor	0.202
Rwork	0.202
RMSD bond length	0.016
RMSD bond angle	3.000 *
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	1.940 *
Rmerge	0.101 *
Total number of observations	70742 *
Number of reflections	33134 *
Completeness [%]	81.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	8.5 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	Tris	100 (mM)	pH8.5
2	1	reservoir	PEG8000	12.5-21 (%(w/v))
3	1	reservoir	lithium sulfate	200 (mM)
4	1	reservoir	sodium azide	1 (mM)