1TPK

CRYSTAL STRUCTURE OF THE KRINGLE-2 DOMAIN OF TISSUE PLASMINOGEN ACTIVATOR AT 2.4-ANGSTROMS RESOLUTION

Experimental procedure

Spacegroup name	P 1 21 1
Unit cell lengths	54.800, 63.580, 46.580
Unit cell angles	90.00, 106.73, 90.00

Refinement procedure

Resolution	10.000 - 2.430 *
R-factor	0.184 *
Rwork	0.184
RMSD bond length	0.016
RMSD bond angle	3.300
Refinement software	X-PLOR

Data quality characteristics

	Overall
Low resolution limit [Å]	10.000 *
High resolution limit [Å]	2.430 *
Rmerge	0.087 *
Number of reflections	7103 *
Completeness [%]	92.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion *	8 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	4 (mg/ml)
2	1	drop		7 (%sat)
3	1	drop		50 (mM)