1TPB
OFFSET OF A CATALYTIC LESION BY A BOUND WATER SOLUBLE
Experimental procedure
Spacegroup name | P 21 21 21 |
Unit cell lengths | 136.400, 74.100, 57.200 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 6.000 - 1.900 |
R-factor | 0.182 |
RMSD bond length | 0.016 |
RMSD bond angle | 0.035 |
Refinement software | PROLSQ |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 11.600 * |
High resolution limit [Å] | 1.900 * |
Rmerge | 0.060 * |
Total number of observations | 137066 * |
Number of reflections | 41619 * |
Completeness [%] | 94.0 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | PGH | 1.5 (M) | 0.0048ml |
2 | 1 | drop | protein | 0.1152ml | |
3 | 1 | reservoir | Tris-HCl | 100 (mM) | |
4 | 1 | reservoir | lithium sulfate | 200 (mM) | |
5 | 1 | reservoir | PEG8000 | 12.5-21 (%) | in 2.5% increments |