1TP7
Crystal Structure of the RNA-dependent RNA Polymerase from Human Rhinovirus 16
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Wavelength(s) | 0.97887 |
Spacegroup name | P 1 21 1 |
格子定数 [Å] | 59.428, 118.890, 183.107 |
格子定数 [度] | 90.00, 96.06, 90.00 |
精密化法
残基 | 50.000 - 2.400 |
R因子 | 0.243 |
Rwork | 0.243 |
R-free | 0.29200 |
Structure solution method | SAD |
結合長の平均二乗偏差(RMSD) [Å] | 0.006 |
結合角の平均二乗偏差(RMSD) [度] | 1.053 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MLPHARE |
Refinement software | CNX |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 50.000 | 2.490 |
分解能 [Å] (高) | 2.400 | 2.400 |
Rmerge_l_obs | 0.090 | 0.463 |
独立反射数 | 98759 | |
<I/σ(I)> | 12.9 | 3 |
完全性 [%] | 99.8 | 99.8 |
冗長性 | 4.5 | 3.9 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, SITTING DROP | 5.6 | 295 | PEG 4000, ammonium sulfate, dimethylbenzylammonium propane sulfonate, sodium citrate, glycerol, dithiothreitol, pH 5.6, VAPOR DIFFUSION, SITTING DROP, temperature 295.0K |