1TOO
Interleukin 1B Mutant F146W
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Collection date | 1999-11-11 |
Detector | RIGAKU RAXIS II |
Wavelength(s) | 1.5418 |
Spacegroup name | P 43 |
Unit cell lengths | 54.950, 54.950, 77.250 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 77.250 - 2.100 |
R-factor | 0.186 |
Rwork | 0.185 |
R-free | 0.19900 |
Structure solution method | MOLECULAR REPLACEMENT |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 77.250 |
High resolution limit [Å] | 2.100 |
Number of reflections | 13286 |
Completeness [%] | 98.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.4 | 298 | 29% AMMONIUM SULFATE W/V, 100 MM Tris , pH 7.4, VAPOR DIFFUSION, HANGING DROP, temperature 298K |