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THE STRUCTURE OF TUMOR NECROSIS FACTOR-ALPHA AT 2.6 ANGSTROMS RESOLUTION. IMPLICATIONS FOR RECEPTOR BINDING

Experimental procedure

Spacegroup name	P 41 21 2
Unit cell lengths	95.000, 95.000, 117.000
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	20.000 * - 2.600
Rwork	0.230
RMSD bond length	0.018 *
RMSD bond angle	4.100
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	2.600 *
Rmerge	0.065 *
Total number of observations	126662 *
Number of reflections	17097 *
Completeness [%]	72.1 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	magnesium sulfate	2.6 (M)