1TLY
Tsx structure
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 8-BM |
Synchrotron site | APS |
Beamline | 8-BM |
Temperature [K] | 100 |
Wavelength(s) | 0.97882 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 149.778, 149.778, 120.888 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.760 - 3.010 |
R-factor | 0.288 |
Rwork | 0.262 |
R-free | 0.28800 |
Structure solution method | SAD |
RMSD bond length | 0.008 |
RMSD bond angle | 1.500 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 49.030 |
High resolution limit [Å] | 3.010 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.3 | 286 | PEG550 27-32%, sodium acetate 50 mM, pH 4.3, VAPOR DIFFUSION, HANGING DROP, temperature 286K |