1TLX
THERMOLYSIN (NATIVE)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 293 |
Detector technology | IMAGE PLATE |
Collection date | 1996-12-01 |
Detector | MAR scanner 300 mm plate |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 93.910, 93.910, 131.170 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 20.000 - 2.100 |
Rwork | 0.153 |
R-free | 0.21400 |
Structure solution method | ISOMORPHOUS REPLACEMENT |
RMSD bond length | 0.014 |
RMSD bond angle | 0.035 |
Data reduction software | DENZO |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.240 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.123 | 0.386 |
Number of reflections | 20252 | |
<I/σ(I)> | 4.9 | 2 |
Completeness [%] | 99.0 | 98 |
Redundancy | 14.9 | 15 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 7.5 | This particular structure is not described in this paper. * |