1TK1
YEAST OXYGEN-DEPENDENT COPROPORPHYRINOGEN OXIDASE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X8C |
Synchrotron site | NSLS |
Beamline | X8C |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-02-13 |
Detector | ADSC QUANTUM 4 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 70.850, 70.850, 114.543 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 59.760 - 1.900 |
R-factor | 0.21713 |
Rwork | 0.215 |
R-free | 0.24907 |
Structure solution method | SAD - CHROMIUM SULFUR ANOMALOUS |
RMSD bond length | 0.021 |
RMSD bond angle | 1.851 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | REFMAC (5.2.0001) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 59.760 | 1.970 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.072 | 0.585 |
Number of reflections | 21772 | |
<I/σ(I)> | 20 | 7 |
Completeness [%] | 96.9 | 95.6 |
Redundancy | 28.7 | 29.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | 294 | 20% PEG 3000, 0.1 M HEPES, 0.2 M sodium acetate, pH 7.5, VAPOR DIFFUSION, SITTING DROP, temperature 294K, pH 7.50 |