1TJ6
Crystal structure of the Xenopus tropicalis Spred1 EVH-1 domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RUH3R |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2004-02-23 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.542 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 32.881, 38.267, 80.226 |
Unit cell angles | 90.00, 95.58, 90.00 |
Refinement procedure
Resolution | 25.000 - 1.650 |
R-factor | 0.1539 |
Rwork | 0.151 |
R-free | 0.18100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1evh |
RMSD bond length | 0.013 |
RMSD bond angle | 1.507 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | 1.690 |
High resolution limit [Å] | 1.650 | 1.650 |
Rmerge | 0.052 | 0.211 |
Number of reflections | 23273 | |
<I/σ(I)> | 38.2 | 9.35 |
Completeness [%] | 96.2 | 94.6 |
Redundancy | 6.2 | 5.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 291 | PEG 3350, potassium fluoride, pH 8, VAPOR DIFFUSION, HANGING DROP, temperature 291K |