1TIS
CRYSTAL STRUCTURE OF THYMIDYLATE SYNTHASE FROM T4 PHAGE
Experimental procedure
Spacegroup name | P 43 21 2 |
Unit cell lengths | 68.020, 68.020, 140.800 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.700 |
R-factor | 0.199 |
Rwork | 0.199 |
RMSD bond length | 0.016 |
RMSD bond angle | 3.800 |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 9999.000 * | |
High resolution limit [Å] | 2.700 * | 2.700 * |
Rmerge | 0.068 * | 0.257 * |
Total number of observations | 30518 * | |
Number of reflections | 6186 * | 192 * |
Completeness [%] | 65.0 * | 12 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 7.5 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | thymidylate synthase from phage T4 | 4.35 (mg/mL) | |
2 | 1 | drop | phosphate | 0.2 (M) | |
3 | 1 | reservoir | ammonium sulfate | 25-30 (%) |