1THJ
CARBONIC ANHYDRASE FROM METHANOSARCINA
Experimental procedure
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL7-1 |
Synchrotron site | SSRL |
Beamline | BL7-1 |
Detector technology | IMAGE PLATE |
Collection date | 1995-07-03 |
Detector | MARRESEARCH |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 71.840, 71.840, 333.513 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 2.800 |
R-factor | 0.234 |
Rwork | 0.234 |
R-free | 0.29500 |
RMSD bond length | 0.013 |
RMSD bond angle | 27.040 * |
Data reduction software | DENZO |
Data scaling software | Agrovata |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | Outer shell | |
High resolution limit [Å] | 2.800 * | |
Rmerge | 0.064 | 0.324 * |
Number of reflections | 21401 | |
Completeness [%] | 95.1 | 82.9 * |
Redundancy | 3 | 2.6 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 6.5 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | ammonium sulfate | 2.0 (M) | |
2 | 1 | 1 | PEG400 | 3 (%) | |
3 | 1 | 2 | cacodylate | 0.1 (M) | |
4 | 1 | 2 | 0.02 (%) |