1THG

1.8 ANGSTROMS REFINED STRUCTURE OF THE LIPASE FROM GEOTRICHUM CANDIDUM

Experimental procedure

Spacegroup name	P 1 21 1
Unit cell lengths	59.400, 84.000, 56.000
Unit cell angles	90.00, 100.10, 90.00

Refinement procedure

Resolution	8.000 * - 1.800
R-factor	0.157
Rwork	0.157
RMSD bond length	0.010
RMSD bond angle	2.400
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	1.800 *
Rmerge	0.039 *
Total number of observations	188971 *
Number of reflections	48512 *
Completeness [%]	96.6 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion *	6 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	N-(carbamoylmethyl)iminodiacetic acid(ADA)
2	1	reservoir	PEG8000	15-18 (%(w/v))