1THC
CRYSTAL STRUCTURE DETERMINATION AT 2.3A OF HUMAN TRANSTHYRETIN-3',5'-DIBROMO-2',4,4',6-TETRA-HYDROXYAURONE COMPLEX
Experimental procedure
Spacegroup name | P 21 21 2 |
Unit cell lengths | 43.402, 85.837, 65.784 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 * - 2.300 |
R-factor | 0.179 |
RMSD bond length | 0.020 |
RMSD bond angle | 3.900 |
Refinement software | PROLSQ |
Data quality characteristics
Overall | |
Rmerge | 0.050 * |
Total number of observations | 18899 * |
Number of reflections | 11830 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Batch method * | 6.9 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | ammonium sulfate | 50 (%sat) | |
2 | 1 | 1 | sodium phosphate | 0.1 (M) |