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1TGK

HUMAN TRANSFORMING GROWTH FACTOR BETA 3, CRYSTALLIZED FROM PEG 4000

Experimental procedure
Detector technologyDIFFRACTOMETER
Collection date1992-12-23
DetectorENRAF-NONIUS FAST
Spacegroup nameP 61 2 2
Unit cell lengths77.800, 77.800, 143.200
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution10.000 - 3.300
R-factor0.228
Rwork0.228
RMSD bond length0.016
RMSD bond angle1.920
Data reduction softwareROTAVATA-AGROVATA
Data scaling softwareCCP4 ((AGROVATA)
Phasing softwareX-PLOR (3.1)
Refinement softwareX-PLOR (3.1)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]9999.000

*

High resolution limit [Å]3.300

*

3.300

*

Rmerge0.132
Number of reflections4232
Completeness [%]100.0100

*

Redundancy9.7
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1Vapor diffusion, hanging drop

*

8.4

*

20-22

*

PEG 4000
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11dropprotein1.5-3 (mg/ml)
21dropacetic acid5 (mM)
31dropPEG400015 (%(w/v))
41dropmagnesium chloride100 (mM)
51dropTris-HCl50 (mM)pH8.4
61reservoirPEG400030 (%(w/v))
71reservoirmagnesium chloride200 (mM)
81reservoirTris-HCl100 (mM)pH8.4

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