1TGC

ON THE DISORDERED ACTIVATION DOMAIN IN TRYPSINOGEN. CHEMICAL LABELLING AND LOW-TEMPERATURE CRYSTALLOGRAPHY

Experimental procedure

Spacegroup name	P 31 2 1
Unit cell lengths	55.110, 55.110, 109.380
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	6.500 * - 1.800
R-factor	0.18 *

Data quality characteristics

	Overall
High resolution limit [Å]	1.800 *
Number of reflections	12067 *
Completeness [%]	65.2 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	10 (mg/ml)
2	1	drop	pancreatic trypsin inhibitor		at a molar ratio of 4-1
3	1	drop		1.5 (M)
4	1	reservoir		1.5 (M)