1TG3

Effect of Shuttle Location and pH Environment on H+ Transfer in Human Carbonic Anhydrase II

Experimental procedure

実験手法	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RU200
Temperature [K]	293
Detector technology	IMAGE PLATE
Detector	RIGAKU RAXIS IV
Wavelength(s)	1.54
Spacegroup name	P 1 21 1
格子定数 [Å]	42.839, 41.629, 72.949
格子定数 [度]	90.00, 104.75, 90.00

精密化法

残基	20.000 - 1.800
Rwork	0.171
R-free	0.20600
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2cba
Data scaling software	SCALEPACK
Phasing software	CNS
Refinement software	CNS

Quality characteristics

	Overall	Outer shell
分解能 [Å] (低)	20.000	1.830
分解能 [Å] (高)	1.800	1.800
独立反射数	22162
完全性 [%]		91.9

結晶化条件

結晶ID	方法	pH	温度	溶液条件
1