1TEN

STRUCTURE OF A FIBRONECTIN TYPE III DOMAIN FROM TENASCIN PHASED BY MAD ANALYSIS OF THE SELENOMETHIONYL PROTEIN

Experimental procedure

Spacegroup name	P 43 21 2
Unit cell lengths	49.780, 49.780, 71.040
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 - 1.800
R-factor	0.196
Rwork	0.196
RMSD bond length	0.012
RMSD bond angle	2.900
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
Low resolution limit [Å]	30.000 *
High resolution limit [Å]	1.800 *
Rmerge	0.067 *
Number of reflections	7950 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	PEG3350	18-22 (%)
2	1	reservoir	citric acid	10 (mM)
3	1	drop	protein	10-20 (mg/ml)