1TEJ
Crystal structure of a disintegrin heterodimer at 1.9 A resolution.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | EMBL/DESY, HAMBURG BEAMLINE X11 |
| Synchrotron site | EMBL/DESY, HAMBURG |
| Beamline | X11 |
| Temperature [K] | 273 |
| Detector technology | CCD |
| Collection date | 2002-12-12 |
| Detector | ENRAF-NONIUS |
| Wavelength(s) | 0.81500 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 90.718, 90.718, 55.477 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 19.960 - 1.900 |
| R-factor | 0.21483 |
| Rwork | 0.213 |
| R-free | 0.25295 |
| Starting model (for MR) | 1rmr |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.408 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | AMoRE |
| Refinement software | REFMAC (5.1.19) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 1.970 |
| High resolution limit [Å] | 1.900 | 1.900 |
| Number of reflections | 18372 | |
| <I/σ(I)> | 10.8 | 2.5 |
| Completeness [%] | 99.9 | 99.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6 | 298 | sodium cacodylate, ammonium sulphate, pH 6.0, VAPOR DIFFUSION, SITTING DROP, temperature 298K |
