1TBQ
CRYSTAL STRUCTURE OF INSECT DERIVED DOUBLE DOMAIN KAZAL INHIBITOR RHODNIIN IN COMPLEX WITH THROMBIN
Experimental procedure
Detector technology | IMAGE PLATE |
Collection date | 1993-12-18 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 91.311, 111.600, 112.140 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 3.100 |
R-factor | 0.175 |
Rwork | 0.175 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.620 |
Data reduction software | MOSFLM |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 999.000 | |
High resolution limit [Å] | 3.100 | 3.100 * |
Rmerge | 0.062 * | |
Total number of observations | 31602 * | |
Number of reflections | 16957 | |
Completeness [%] | 79.1 * | 82.3 * |
Redundancy | 1.86 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 6 * | 20 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | PEG4000 | 10 (%) | |
2 | 1 | reservoir | phosphate | 300 (mM) |