1TBE

STRUCTURE OF TETRAUBIQUITIN SHOWS HOW MULTIUBIQUITIN CHAINS CAN BE FORMED

Experimental procedure

Spacegroup name	P 1 21 1
Unit cell lengths	24.100, 57.000, 47.000
Unit cell angles	90.00, 94.06, 90.00

Refinement procedure

Resolution	6.000 * - 2.400
R-factor	0.184
Rwork	0.184
RMSD bond length	0.015
RMSD bond angle	2.500
Phasing software	X-PLOR
Refinement software	PROLSQ

Data quality characteristics

	Overall
High resolution limit [Å]	2.400 *
Rmerge	0.093 *
Total number of observations	21877 *
Number of reflections	4821 *
Completeness [%]	95.9 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	PEG4000	20 (%)
2	1	drop	ammonium acetate	0.2 (M)
3	1	reservoir	acetate	0.1 (M)