1TAU
TAQ POLYMERASE (E.C.2.7.7.7)/DNA/B-OCTYLGLUCOSIDE COMPLEX
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X12C |
Synchrotron site | NSLS |
Beamline | X12C |
Temperature [K] | 110 |
Detector technology | IMAGE PLATE |
Collection date | 1995-06-01 |
Detector | MARRESEARCH |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 107.600, 107.600, 170.010 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 8.000 - 3.000 |
Rwork | 0.244 |
R-free | 0.30500 |
RMSD bond length | 0.009 |
RMSD bond angle | 22.300 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 3.000 |
Rmerge | 0.088 |
Number of reflections | 21866 |
<I/σ(I)> | 8.9 |
Completeness [%] | 93.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 22 * | pH 6.00, VAPOR DIFFUSION, HANGING DROP, temperature 295.00K |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | ||
2 | 1 | 1 | PEG 8000 | ||
3 | 1 | 1 | NA CITRATE | ||
4 | 1 | 1 | ZN SULFATE |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | sodium citrate | 100 (mM) | |
2 | 1 | drop | PEG8000 | 4 (%(w/v)) | |
3 | 1 | drop | 1 (mM) | ||
4 | 1 | drop | 0-400 (mM) |