1TAT

CRYSTALLINE MITOCHONDRIAL ASPARTATE AMINOTRANSFERASE EXISTS IN ONLY TWO CONFORMATIONS

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	69.500, 89.600, 144.700
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	15.000 - 3.000
R-factor	0.15
RMSD bond length	0.020
RMSD bond angle	3.100
Refinement software	TNT

Data quality characteristics

	Overall	Outer shell
High resolution limit [Å]	3.000 *	3.000 *
Rmerge	0.105 *
Total number of observations	65983 *
Number of reflections	18194 *
Completeness [%]	97.0 *	88 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion *	7.5 *	4 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	PEG4000	19-21 (%(w/v))
2	1	drop	asparatate aminotransferase	10-12 (mg/ml)