1T9M
X-ray crystal structure of phzG from pseudomonas aeruginosa
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 105 |
Detector technology | IMAGE PLATE |
Collection date | 2003-03-21 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 63.590, 69.020, 89.080 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.900 |
R-factor | 0.18604 |
Rwork | 0.184 |
R-free | 0.23103 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1dnl |
RMSD bond length | 0.025 |
RMSD bond angle | 1.954 |
Data reduction software | CrystalClear ((MSC/RIGAKU)) |
Data scaling software | d*TREK |
Phasing software | CNS |
Refinement software | REFMAC (5.1.27) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 54.000 | 1.970 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.038 | 0.159 |
Number of reflections | 31579 | |
<I/σ(I)> | 19 | 5.3 |
Completeness [%] | 99.7 | 99.9 |
Redundancy | 6 | 6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 298 | 0.2M lithium sulfate, 0.1M tris, 25% (w/v) PEG 3350, pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |