1T8X
r106g kdo8ps with pep and a5p
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS IV |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 84.375, 84.375, 160.459 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 54.020 - 1.800 |
Rwork | 0.197 |
R-free | 0.24200 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 1fww |
RMSD bond length | 0.009 |
RMSD bond angle | 1.500 |
Data reduction software | CrystalClear ((MSC/RIGAKU)) |
Data scaling software | d*TREK |
Phasing software | CNS |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 54.020 |
High resolution limit [Å] | 1.800 |
Number of reflections | 60408 |
<I/σ(I)> | 4.5 |
Completeness [%] | 96.6 |
Redundancy | 9.12 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.7 | 277 | PEG, Na-acetate, pH 4.7, VAPOR DIFFUSION, HANGING DROP, temperature 277K |