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1T6Y

Crystal structure of ADP, AMP, and FMN bound TM379

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsALS BEAMLINE 5.0.1
Synchrotron siteALS
Beamline5.0.1
Temperature [K]90
Detector technologyCCD
Collection date2001-11-10
DetectorADSC QUANTUM 4
Wavelength(s)1.0000
Spacegroup nameP 1 21 1
Unit cell lengths67.803, 82.661, 66.717
Unit cell angles90.00, 116.42, 90.00
Refinement procedure
Resolution19.920 - 2.800
R-factor0.2311
Rwork0.231
R-free0.29800
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.011
RMSD bond angle1.600
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareCNS
Refinement softwareCNS
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.0002.900
High resolution limit [Å]2.8002.800
Number of reflections16249
Completeness [%]99.397.8
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7.5298PEG 4000, sodium citrate, glycerol, propanol, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K

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