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1T6N

Crystal structure of the N-terminal domain of human UAP56

Experimental procedure
Experimental methodMAD
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 19-ID
Synchrotron siteAPS
Beamline19-ID
Temperature [K]100
Detector technologyCCD
Collection date2003-10-10
Wavelength(s)0.97921, 0.97923, 0.96417
Spacegroup nameP 1 21 1
Unit cell lengths49.453, 47.284, 87.190
Unit cell angles90.00, 98.23, 90.00
Refinement procedure
Resolution30.000 - 1.940
R-factor0.216
Rwork0.216
R-free0.25500
Structure solution methodMAD
RMSD bond length0.007
RMSD bond angle1.340
Data reduction softwareHKL-2000
Data scaling softwareSCALEPACK
Phasing softwareSOLVE
Refinement softwareCNS
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.0002.010
High resolution limit [Å]1.9401.940
Rmerge0.0600.450
Number of reflections29132
<I/σ(I)>25.55.4
Completeness [%]98.7
Redundancy5.14.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP5.6291sodium citrate, PEG MME 2000, pH 5.6, VAPOR DIFFUSION, HANGING DROP, temperature 291K
1VAPOR DIFFUSION, HANGING DROP5.6291sodium citrate, PEG MME 2000, pH 5.6, VAPOR DIFFUSION, HANGING DROP, temperature 291K
1VAPOR DIFFUSION, HANGING DROP5.6291sodium citrate, PEG MME 2000, pH 5.6, VAPOR DIFFUSION, HANGING DROP, temperature 291K

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