1T4Q

Interleukin 1 beta F101W

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU
Temperature [K]	298
Detector technology	IMAGE PLATE
Collection date	2000-02-01
Detector	RIGAKU RAXIS II
Wavelength(s)	1.5418
Spacegroup name	P 43
Unit cell lengths	55.110, 55.110, 76.720
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	55.110 - 2.100
R-factor	0.1837
Rwork	0.182
R-free	0.20880
Structure solution method	MOLECULAR REPLACEMENT
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	CNS
Refinement software	CNS

Data quality characteristics

	Overall
Low resolution limit [Å]	55.110
High resolution limit [Å]	2.100
Number of reflections	13419
Completeness [%]	99.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7.4	298	29% AMMONIUM SULFATE W/V, 100 MM, pH 7.4, VAPOR DIFFUSION, HANGING DROP, temperature 298K