1T4Q
Interleukin 1 beta F101W
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Collection date | 2000-02-01 |
Detector | RIGAKU RAXIS II |
Wavelength(s) | 1.5418 |
Spacegroup name | P 43 |
Unit cell lengths | 55.110, 55.110, 76.720 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 55.110 - 2.100 |
R-factor | 0.1837 |
Rwork | 0.182 |
R-free | 0.20880 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 55.110 |
High resolution limit [Å] | 2.100 |
Number of reflections | 13419 |
Completeness [%] | 99.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.4 | 298 | 29% AMMONIUM SULFATE W/V, 100 MM, pH 7.4, VAPOR DIFFUSION, HANGING DROP, temperature 298K |